N-苄基-N,alpha,alpha,alpha-四甲基硅烷胺合成路线 （共 3 条）
反应条件
1: benzyl-methyl-amine With n-butyllithium in diethyl ether; hexane T=-78 - -60°C; 1 h; Inert atmosphere; 2: chloro-trimethyl-silane in diethyl ether; hexane T=-70 - 20°C; Inert atmosphere;
参考文献
OMEGACHEM INC.; COUTURIER, Michel; L'HEUREUX, Alexandre
Patent: WO2010/145037 A1, 2010 ;
Location in patent: Page/Page column 29-30 ;
反应条件
in acetonitrile Heating;
参考文献
Diekman,J. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3904 - 3919
反应条件
thionyl chloride in diethyl ether
T=-78°C;
参考文献
Neidlein, Richard; Walser, Peter
Chemische Berichte, 1982 , vol. 115, # 7 p. 2428 - 2436
