diethyl benzenedicarboxylate; copper

暂无反应条件数据

<b>Multi-step reaction with 3 steps<br /> </b>1: 12 percent / O-mesitylenesulfonylhydroxylamine / CH₂Cl₂ / 20 &deg;C<br />2: 65 percent / diethyl ether / 24 h / Heating<br />3: 57 percent / O-mesitylenesulfonylhydroxylamine / CH₂Cl₂ / 20 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 26 percent / O-mesitylenesulfonylhydroxylamine / CH₂Cl₂ / 20 &deg;C<br />2: 65 percent / diethyl ether / 24 h / Heating<br />3: 57 percent / O-mesitylenesulfonylhydroxylamine / CH₂Cl₂ / 20 &deg;C<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '507540', constants.ctx, '0')">nitrobenzene</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '956581', constants.ctx, '0')">trichlorophosphate</a> <br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 65 percent / diethyl ether / 24 h / Heating<br />2: 57 percent / O-mesitylenesulfonylhydroxylamine / CH₂Cl₂ / 20 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: potassium <i>tert</i>-butylate / 1-methyl-pyrrolidin-2-one / 200 &deg;C / |Microwave irradiation<br />2: 1-methyl-pyrrolidin-2-one / 200 &deg;C / |Microwave irradiation<br />3: 1-methyl-pyrrolidin-2-one / 200 &deg;C / |Microwave irradiation<br /> <br /> &nbsp;