2,4,5-三甲氧基甲苯合成路线 （共 13 条）
反应条件
potassium carbonate in acetone T=75°C; 72 h; sealed tube;
参考文献
Kozlova, I. V.; Obol'nikova, E. A.; Chupina, L. N.; Bekker, A. R.; Samokhvalov, G. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 296 - 299
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 2 p. 351 - 354
反应条件
NiRa in ethanol 2 h; Heating;
参考文献
Cabiddu, Salvatore; Contini, Liliana; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna
Tetrahedron, 1991 , vol. 47, # 44 p. 9279 - 9288
反应条件
cesium fluoride in water; N,N-dimethyl-formamide 24 h; Heating;
参考文献
Cabiddu, Salvatore; Contini, Liliana; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna
Tetrahedron, 1991 , vol. 47, # 44 p. 9279 - 9288
反应条件
potassium carbonate in acetone T=75°C; 72 h; sealed tube;
参考文献
Kozlova, I. V.; Obol'nikova, E. A.; Chupina, L. N.; Bekker, A. R.; Samokhvalov, G. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 296 - 299
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 2 p. 351 - 354
反应条件
2: 75 percent / CsF / dimethylformamide; H2O / 24 h / Heating 3: 78 percent / Ni/Ra / ethanol / 2 h / Heating View Scheme
参考文献
Cabiddu, Salvatore; Contini, Liliana; Fattuoni, Claudia; Floris, Costantino; Gelli, Gioanna
Tetrahedron, 1991 , vol. 47, # 44 p. 9279 - 9288
反应条件
1: 45.2 percent / TiCl4 / CH2Cl2 / 3 h / 20 °C 2: 73.7 percent / 30percent NaOH / ethanol / 3 h / Heating 3: 76.2 percent / perbenzoic acid / CH2Cl2 / 3 h / Heating 4: 76.44 percent / K2CO3 / acetone / 72 h / 75 °C / sealed tube View Scheme
参考文献
Kozlova, I. V.; Obol'nikova, E. A.; Chupina, L. N.; Bekker, A. R.; Samokhvalov, G. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 296 - 299
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 2 p. 351 - 354
反应条件
1: 76.2 percent / perbenzoic acid / CH2Cl2 / 3 h / Heating 2: 76.44 percent / K2CO3 / acetone / 72 h / 75 °C / sealed tube View Scheme
参考文献
Kozlova, I. V.; Obol'nikova, E. A.; Chupina, L. N.; Bekker, A. R.; Samokhvalov, G. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 296 - 299
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 2 p. 351 - 354
反应条件
1: 73.7 percent / 30percent NaOH / ethanol / 3 h / Heating 2: 76.2 percent / perbenzoic acid / CH2Cl2 / 3 h / Heating 3: 76.44 percent / K2CO3 / acetone / 72 h / 75 °C / sealed tube View Scheme
参考文献
Kozlova, I. V.; Obol'nikova, E. A.; Chupina, L. N.; Bekker, A. R.; Samokhvalov, G. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 296 - 299
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 2 p. 351 - 354
反应条件
1: hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 0.12 h / Irradiation 2: KOH / bis-(2-hydroxy-ethyl) ether / 0.28 h / Irradiation View Scheme
参考文献
Chattopadhyay, Sarmishtha; Banerjee, Sajal Kumar; Mitra, Alok Kumar
Journal of the Indian Chemical Society, 2002 , vol. 79, # 11 p. 906 - 907
反应条件
potassium hydroxide T=-10°C;
参考文献
Luff; Perkin; Robinson
Journal of the Chemical Society, 1910 , vol. 97, p. 1139
