4-[2-(苯基磺酰基)乙基]苯胺合成路线 （共 4 条）
反应条件
ammonium formate; palladium 10 on activated carbon in tetrahydrofuran; methanol T=20°C; 2 h;
参考文献
Ashcroft, Christopher P.; Pettman, Alan; Watkinson, Simon; Hellier, Paul
Organic Process Research and Development, 2011 , vol. 15, # 1 p. 98 - 103
反应条件
1: water; isopropyl alcohol / 42 h / 70 °C 2: 5 Pd(II)/C(eggshell); hydrogen / methanol / 18 h / 60 °C / 3102.97 Torr View Scheme
参考文献
Ashcroft, Christopher P.; Pettman, Alan; Watkinson, Simon; Hellier, Paul
Organic Process Research and Development, 2011 , vol. 15, # 1 p. 98 - 103
反应条件
1: water; isopropyl alcohol / 42 h / 70 °C 2: 5 Pd(II)/C(eggshell); hydrogen / methanol / 18 h / 60 °C / 3102.97 Torr View Scheme
参考文献
Ashcroft, Christopher P.; Pettman, Alan; Watkinson, Simon; Hellier, Paul
Organic Process Research and Development, 2011 , vol. 15, # 1 p. 98 - 103
反应条件
1.1: sulfuric acid; sodium nitrite / water; acetonitrile / 1 h / 4 °C 1.2: 4 - 20 °C 2.1: calcium chloride; potassium hydroxide / water; acetonitrile 3.1: sulfuric acid / water; acetonitrile / 16 h / 80 °C View Scheme
参考文献
Ashcroft, Christopher P.; Pettman, Alan; Watkinson, Simon; Hellier, Paul
Organic Process Research and Development, 2011 , vol. 15, # 1 p. 98 - 103
