7-(2,5-二羟基-3,4,6-三甲基苯基)-7-苯基庚酸合成路线 （共 5 条）
反应条件
boron trifluoride diethyl etherate in toluene T=60°C; 2 h;
参考文献
Kuninobu, Yoichiro; Kawata, Atsushi; Noborio, Taihei; Yamamoto, Syun-Ichi; Matsuki, Takashi; Takata, Kazumi; Takai, Kazuhiko
Chemistry - An Asian Journal, 2010 , vol. 5, # 4 p. 941 - 945
反应条件
1: AlCl3 / 2 h / 90 °C 2: NaBH4 / methanol / 0.5 h / 0 °C 3: 95 percent / 2.5 N NaOH / tetrahydrofuran / 3 h / 70 °C 4: boron trifluoride etherate / toluene / 2 h / 60 °C View Scheme
参考文献
Shiraishi; Kato; Terao; Ashida; Terashita; Kito
Journal of Medicinal Chemistry, 1989 , vol. 32, # 9 p. 2214 - 2221
反应条件
1: 98 percent / SOCl2 / CH2Cl2 / 2 h / 50 °C 2: AlCl3 / 2 h / 90 °C 3: NaBH4 / methanol / 0.5 h / 0 °C 4: 95 percent / 2.5 N NaOH / tetrahydrofuran / 3 h / 70 °C 5: boron trifluoride etherate / toluene / 2 h / 60 °C View Scheme
参考文献
Shiraishi; Kato; Terao; Ashida; Terashita; Kito
Journal of Medicinal Chemistry, 1989 , vol. 32, # 9 p. 2214 - 2221
反应条件
1: NaBH4 / methanol / 0.5 h / 0 °C 2: 95 percent / 2.5 N NaOH / tetrahydrofuran / 3 h / 70 °C 3: boron trifluoride etherate / toluene / 2 h / 60 °C View Scheme
参考文献
Shiraishi; Kato; Terao; Ashida; Terashita; Kito
Journal of Medicinal Chemistry, 1989 , vol. 32, # 9 p. 2214 - 2221
反应条件
iron(III) chloride in tetrahydrofuran 0.5 h; Ambient temperature; Yield given;
参考文献
Kuninobu, Yoichiro; Kawata, Atsushi; Noborio, Taihei; Yamamoto, Syun-Ichi; Matsuki, Takashi; Takata, Kazumi; Takai, Kazuhiko
Chemistry - An Asian Journal, 2010 , vol. 5, # 4 p. 941 - 945
