Cadmium acetate in 1,4-dioxane
T=180°C; P=12920 Torr; 3 h;
参考文献
Abramova, N. D.; Afonin, A. V.; Naumova, G. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 2 p. 223 - 224
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , # 2 p. 270 - 271
1: 1-chloro-1,1-difluoro-methane With potassium hydroxide in ethylene glycol dimethyl ether; water
0.166667 h;
2: 2-mercaptobenzothiazole in ethylene glycol dimethyl ether; water
T=20°C; Inert atmosphere;
tert.-butylhydroperoxide; trifluoroacetic acid in dichloromethane; water
T=23°C; 16 h; regioselective reaction;
参考文献
Fujiwara, Yuta; Dixon, Janice A.; Rodriguez, Rodrigo A.; Baxter, Ryan D.; Dixon, Darryl D.; Collins, Michael R.; Blackmond, Donna G.; Baran, Phil S.
Journal of the American Chemical Society, 2012 , vol. 134, # 3 p. 1494 - 1497
