3-O-(叔丁基二甲基硅烷氧)-2-Fmoc-赤-鞘氨醇合成路线 （共 2 条）
反应条件
1: tetrazole / CH2Cl2; acetonitrile / 0.5 h 2: iodine, pyridine, water / CH2Cl2 3: 95 percent / 33percent HNMe2 / ethanol / 72 h / 45 °C 4: 75 percent / tetrabutylammonium fluoride / tetrahydrofuran / 72 h / 45 °C View Scheme
参考文献
Kratzer, Bernd; Schmidt, Richard R.
Tetrahedron Letters, 1993 , vol. 34, # 11 p. 1761 - 1764
反应条件
Multi-step reaction with 2 steps 1: 91 percent / Ph3P, H2O, pyridine2: 92 percent / NaHCO3 / dioxane; H2O
参考文献
Kratzer, Bernd; Schmidt, Richard R. Tetrahedron Letters, 1993 , vol. 34, # 11 p. 1761 - 1764
