苯基(1-甲基丙基)硫醚合成路线 （共 33 条）
反应条件
1: KHSO4
2: NaOMe
3: KOtBu
4: KOtBu
5: H2 / Raney-Ni
View Scheme
参考文献
Parham,W.E. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 509 - 515
反应条件
1: KOtBu
2: KOtBu
3: H2 / Raney-Ni
View Scheme
参考文献
Parham,W.E. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 509 - 515
参考文献
Parham,W.E. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 509 - 515
反应条件
1: KOtBu
2: H2 / Raney-Ni
View Scheme
参考文献
Parham,W.E. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 509 - 515
参考文献
Liu, Bo; Shine, Henry J.
Journal of Physical Organic Chemistry, 2001 , vol. 14, # 2 p. 81 - 89
反应条件
sec.-butyllithium
1.) THF, -78 deg C, 0.5 h, 2.) 0 deg C, 5 h, 3.) methyl iodide, 0.5 h, -23 deg C, water; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Cohen, Theodore; Yu, Lin-Chen
Journal of Organic Chemistry, 1984 , vol. 49, # 4 p. 605 - 608
反应条件
triethylsilane; water; titanium tetrachloride
1.) CH2Cl2, -78 deg C, 0.5 h, 2.) CH2Cl2; Yield given. Multistep reaction;
参考文献
Takeda, Takeshi; Tsuchida, Toshio; Fujiwara, Tooru
Chemistry Letters, 1984 , p. 1219 - 1220
反应条件
n-butyllithium; potassium tert-butylate
1.) hexane, from -20 deg C to -10 deg C, 4 h, 2.) hexane, RT, overnight; Yield given. Multistep reaction;
参考文献
Cabiddu, S.; Fattuoni, C.; Floris, C.; Gelli, G.; Melis, S.
Journal of Organometallic Chemistry, 1992 , vol. 441, # 2 p. 197 - 202
参考文献
Manoharan, Muthiah; Eliel, Ernest L.
Magnetic Resonance in Chemistry, 1985 , vol. 23, # 4 p. 225 - 231
反应条件
lithium aluminium tetrahydride; bromine
1) THF, 0 deg C, 2) chlorobenzene, reflux, 3) chlorobenzene, H2O, 24 h, reflux; Product distribution;
参考文献
Kauffmann, Thomas; Joussen, Rolf; Woltermann, Annegret
Chemische Berichte, 1986 , vol. 119, # 7 p. 2135 - 2142
