2-(4-氯苯基)-3-硝基丙烷-1-胺合成路线 （共 3 条）
反应条件
1: 72 percent / 1,1,3,3-tetramethylguanidine / tetrahydrofuran / 96 h 2: 96 percent / 50percent KOH / methanol / 1 h 3: SOCl2 / 1 h / Heating 4: NaN3 / H2O; acetone / 0.83 h 5: CF3COOH / CH2Cl2 / Heating 6: K2CO3 / H2O; methanol / 72 h / Ambient temperature View Scheme
参考文献
Abbenante, Giovanni; Hughes, Robert; Prager, Rolf H.
Australian Journal of Chemistry, 1994 , vol. 47, # 8 p. 1441 - 1452
反应条件
1: SOCl2 / 1 h / Heating 2: NaN3 / H2O; acetone / 0.83 h 3: CF3COOH / CH2Cl2 / Heating 4: K2CO3 / H2O; methanol / 72 h / Ambient temperature View Scheme
参考文献
Abbenante, Giovanni; Hughes, Robert; Prager, Rolf H.
Australian Journal of Chemistry, 1994 , vol. 47, # 8 p. 1441 - 1452
反应条件
1: 96 percent / 50percent KOH / methanol / 1 h 2: SOCl2 / 1 h / Heating 3: NaN3 / H2O; acetone / 0.83 h 4: CF3COOH / CH2Cl2 / Heating 5: K2CO3 / H2O; methanol / 72 h / Ambient temperature View Scheme
参考文献
Abbenante, Giovanni; Hughes, Robert; Prager, Rolf H.
Australian Journal of Chemistry, 1994 , vol. 47, # 8 p. 1441 - 1452
