2,3-二氯-5,8-二羟基-1,4-萘醌合成路线 （共 17 条）
反应条件
aluminum oxide; potassium fluoride Heating;
参考文献
Anufriev, Victor Ph.; Novikov, Vyacheslav L.
Tetrahedron Letters, 1995 , vol. 36, # 14 p. 2515 - 2518
反应条件
aluminum oxide; cesium fluoride 1 h; Heating;
参考文献
Pokhilo, Nataly D.; Shuvalova, Maria I.; Lebedko, Maxim V.; Sopelnyak, Galina I.; Yakubovskaya, Alia Ya.; Mischenko, Natalia P.; Fedoreyev, Sergey A.; Anufriev, Victor Ph.
Journal of Natural Products, 2006 , vol. 69, # 8 p. 1125 - 1129
反应条件
aluminum oxide; potassium fluoride
Heating;
参考文献
Anufriev, Victor Ph.; Novikov, Vyacheslav L.
Tetrahedron Letters, 1995 , vol. 36, # 14 p. 2515 - 2518
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in acetone
1 h; Ambient temperature;
参考文献
Horowska; Mazerska; Ledochowski; Cristalli; Franchetti; Martelli
European Journal of Medicinal Chemistry, 1988 , vol. 23, # 1 p. 91 - 96
反应条件
1.1: tin(ll) chloride; hydrogenchloride / water / 5 h / 140 °C
2.1: potassium hydride / N,N-dimethyl-formamide / -35 - 40 °C / |Inert atmosphere
2.2: |Inert atmosphere
3.1: trichlorophosphate / chloroform / 8 h / |Reflux
View Scheme
参考文献
Guerrero-Vasquez, Guillermo A.; Andrade, Carlos Kleber Z.; Molinillo, Jose M. G.; MacIas, Francisco A.
European Journal of Organic Chemistry, 2013 , # 27 p. 6175 - 6180
反应条件
hydrogenchloride; tin(ll) chloride
5 h; Heating;
参考文献
Nicolaou; Hepworth, David
Angewandte Chemie - International Edition, 1998 , vol. 37, # 6 p. 839 - 841
反应条件
1: 66 percent / MnO2, conc. H2SO4 / 2 h / Ambient temperature
2: 40 percent / 2-methyl-propan-2-ol / Heating
3: 81 percent / 3 h / Heating
4: 74 percent / CsF, Al2O3 / 8 h / 90 - 95 °C
5: 91 percent / AlCl3 / nitrobenzene / 4 h / 80 °C
View Scheme
参考文献
Anufriev, Victor Ph.; Novikov, Vyacheslav L.; Maximov, Oleg B.; Elyakov, George B.; Levitsky, Dmitry O.; Lebedev, Alexander V.; Sadretdinov, Safa M.; Shvilkin, Alexei V.; Afonskaya, Natalya I.; Ruda, Mikhail Ya.; Cherpachenko, Nina M.
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 6 p. 587 - 592
