N-乙酰基-L-缬氨酸甲酯合成路线 （共 18 条）
反应条件
4-methyl-morpholine in chloroform
参考文献
Sugawara, Neal; Stevens, E. S.; Bonora, G. M.; Toniolo, C.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7044 - 7047
反应条件
in dichloromethane T=20°C; 4 h;
参考文献
De Marco, Rosaria; Gioia, Maria Luisa Di; Leggio, Antonella; Liguori, Angelo; Viscomi, Maria Caterina
European Journal of Organic Chemistry, 2009 , # 22 p. 3795 - 3800
反应条件
sulfated tungstate in toluene 18 h; RefluxGreen chemistry;
参考文献
Pathare, Sagar P.; Jain, Ashish Kumar H.; Akamanchi, Krishnacharya G.
RSC Advances, 2013 , vol. 3, # 21 p. 7697 - 7703
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Rella, Maria Rosaria; Williard, Paul G.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 525 - 531
反应条件
1: 2.462 g / Et3N / CH2Cl2 2: H2O; Acylase I on Eupergit C / 27 h / 25 °C View Scheme
参考文献
Liljeblad, Arto; Aksela, Reijo; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2001 , vol. 12, # 14 p. 2059 - 2066
反应条件
1: SOCl2 2: 2.462 g / Et3N / CH2Cl2 3: H2O; Acylase I on Eupergit C / 27 h / 25 °C View Scheme
参考文献
Liljeblad, Arto; Aksela, Reijo; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2001 , vol. 12, # 14 p. 2059 - 2066
反应条件
1: mercaptoacetic acid; triethylamine / 0.08 h / 20 °C / |Ionic liquid 2: dichloromethane; water / 4 h / 20 °C / |Alkaline conditions View Scheme
参考文献
Di Gioia; Barattucci; Bonaccorsi; Leggio; Minuti; Romio; Temperini; Siciliano
RSC Advances, 2014 , vol. 4, # 6 p. 2678 - 2686
反应条件
Acylase I on Eupergit C; water T=25°C; 27 h;
参考文献
Liljeblad, Arto; Aksela, Reijo; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2001 , vol. 12, # 14 p. 2059 - 2066
反应条件
pyridine; sodium acetate
参考文献
Reihlen; Knoepfle
Justus Liebigs Annalen der Chemie, 1936 , vol. 523, p. 199,203
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Bickley, Jamie F.; Roberts, Stanley M.; Runhui, Ye; Skidmore, John; Smith, Corina B.
Tetrahedron, 2003 , vol. 59, # 30 p. 5731 - 5736
