2,6-二甲基苯甲酸甲酯合成路线 （共 33 条）
反应条件
tributyl-amine in N,N-dimethyl-formamide T=285°C; P=112511 Torr; 0.05 h;
参考文献
Glasnov, Toma N.; Kappe, C. Oliver; Holbrey, John D.; Seddon, Kenneth R.; Yan, Ting
Green Chemistry, 2012 , vol. 14, # 11 p. 3071 - 3076,6
反应条件
potassium carbonate in acetone T=20°C; 4 h;
参考文献
Hardin, Alison R.; Sarpong, Richmond
Organic Letters, 2007 , vol. 9, # 22 p. 4547 - 4550
反应条件
sulfuric acid anschliessend Behandeln mit Methanol;
参考文献
Journal of the American Chemical Society, , vol. 75, p. 20,23
参考文献
Chemische Berichte, , vol. 108, p. 1694 - 1711
反应条件
triethylamine in methanol; dichloromethane; N,N-dimethyl-formamide
反应条件
18-crown-6 ether; potassium carbonate T=90 - 150°C; 2 h;
参考文献
Renga, James M.; Wang, Pen-Chung
Synthetic Communications, 1984 , vol. 14, # 1 p. 77 - 82
反应条件
1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in dimethyl sulfoxide T=70°C; 2 h;
参考文献
Dolle, Roland E.; Schmidt, Stanley J.; Kruse, Lawrence I.
Journal of the Chemical Society, Chemical Communications, 1987 , # 12 p. 904 - 905
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate in 1-methyl-pyrrolidin-2-one T=100°C; P=3750.38 Torr; 24 h; Inert atmosphereAutoclave; Reagent/catalyst; chemoselective reaction;
参考文献
Barnard, Christopher F.J.
Organic Process Research and Development, 2008 , vol. 12, # 4 p. 566 - 574
反应条件
C44H34Br2P2Pd; potassium carbonate in 1-methyl-pyrrolidin-2-one T=100°C; P=3750.38 Torr; 24 h; Inert atmosphereAutoclave; Reagent/catalyst; chemoselective reaction;
参考文献
Organic Process Research and Development, , vol. 12, # 4 p. 566 - 574
反应条件
C27H50Cl2P2Pd; potassium carbonate in 1-methyl-pyrrolidin-2-one T=120°C; P=1500.15 Torr; 24 h; Inert atmosphereAutoclave; Reagent/catalyst; chemoselective reaction;
参考文献
Organic Process Research and Development, , vol. 12, # 4 p. 566 - 574
