2,6-二甲基苯甲酸甲酯合成路线 （共 33 条）
反应条件
trifluoroacetic anhydride
参考文献
Journal of the American Chemical Society, , vol. 77, p. 3403
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Journal of Medicinal Chemistry, , vol. 42, # 10 p. 1789 - 1802
反应条件
1.1: Zn; TiCl4 / tetrahydrofuran / 14 h / 4 °C 1.2: 85 percent / tetrahydrofuran / 0.5 h / 20 °C 2.1: 30 percent Chromat. / silica / 0.67 h / 700 °C / 0.01 Torr View Scheme
参考文献
Australian Journal of Chemistry, , vol. 53, # 5 p. 435 - 437
反应条件
1: 2,6-t-butyl-4-methylpyridine / CHCl3 / 12 h / Heating 2: 87 percent Chromat. / triethylamine, 1,3-bis(diphenylphosphino)propane, / Pd(OAc)2 / dimethylsulfoxide / 2 h / 70 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 904 - 905
参考文献
Heterocycles, , vol. 25, p. 117 - 121
反应条件
1: 50 percent / HBr / diazotization 2: 1.) Mg / 1.) ether, 2.) ether, reflux, 2 h; room temp., overnight View Scheme
参考文献
Monatshefte fur Chemie, , vol. 127, # 2 p. 185 - 200
参考文献
Journal of the American Chemical Society, , vol. 90, p. 4410 - 4413
Recueil des Travaux Chimiques des Pays-Bas, , vol. 79, p. 1211 - 1222
Journal of the American Chemical Society, , vol. 76, p. 787,788
Magnetic Resonance in Chemistry, , vol. 42, # 10 p. 844 - 851
反应条件
1: (i) Mg, (ii) /BRN= 1900390/ View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 79, p. 1211 - 1222
反应条件
magnesium 1.) ether, 2.) ether, reflux, 2 h; room temp., overnight; Yield given. Multistep reaction;
参考文献
Monatshefte fur Chemie, , vol. 127, # 2 p. 185 - 200
反应条件
48 h; Ambient temperature; Product distribution;
参考文献
Jung, Michael E.; Hagenah, Jeffrey A.
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 1889 - 1902
