反应条件
hydrogen in chloroform dry solvents; degassing mixt. of Mo-compd./Ph2CHCN dissolved in CHCl3, placing under H2 (600 Torr at -196°C), stirring at 50°C, frozing mixt. at -196°C, addn. of acid, stirring under H2 (600 Torr), total react. time 3 days; filtration, crystn. by addn. of Et2O, recrystn. (MeCN/Et2O), drying in vac.;
参考文献
Organometallics, , vol. 9, p. 1607 - 1617
