1: 63 percent / dimethylformamide; CH2Cl2 / 24 h 2: aq. NaOH / methanol / 0.5 h / 0 °C View Scheme
参考文献
Egholm, Michael; Behrens, Carsten; Christensen, Leif; Berg, Rolf H.; Nielsen, Peter E.; Buchardt, Ole
Journal of the Chemical Society, Chemical Communications, 1993 , # 9 p. 800 - 801
1: 63 percent / dimethylformamide; CH2Cl2 / 24 h 2: aq. NaOH / methanol / 0.5 h / 0 °C View Scheme
参考文献
Egholm, Michael; Behrens, Carsten; Christensen, Leif; Berg, Rolf H.; Nielsen, Peter E.; Buchardt, Ole
Journal of the Chemical Society, Chemical Communications, 1993 , # 9 p. 800 - 801
1: 73 percent / NaH / dimethylformamide / 1.) r.t., 2 h, 2.) r.t., 2 h 2: 63 percent / dimethylformamide; CH2Cl2 / 24 h 3: aq. NaOH / methanol / 0.5 h / 0 °C View Scheme
参考文献
Egholm, Michael; Behrens, Carsten; Christensen, Leif; Berg, Rolf H.; Nielsen, Peter E.; Buchardt, Ole
Journal of the Chemical Society, Chemical Communications, 1993 , # 9 p. 800 - 801
1.1: caesium carbonate; potassium carbonate / N,N-dimethyl-formamide / 0.08 h 1.2: 2.5 h / 20 °C 2.1: potassium hydroxide; water / methanol / 0.75 h / 20 °C View Scheme
参考文献
Friedrich, Peter; Baisch, Ulrich; Harrington, Ross W.; Lyatuu, Fredrick; Zhou, Kai; Zelder, Felix; McFarlane, William; Buckel, Wolfgang; Golding, Bernard T.
Chemistry - A European Journal, 2012 , vol. 18, # 50 p. 16114 - 16122
