反应条件
in pentane
byproducts: (C6F5S)3P; addn. of PCl5 to a suspension of the Pb-compd. in pentane at 0°C and allowing the mixt. to warm to room temp.; sepn. of the pptd. Pb-compd. by filtn., concg. of the remainin soln. at reduced pressure, pptn. of the disulfide upon cooling, sepn. by filtn., obtaining the thiophosphite after concg. the filtrate;
参考文献
Denney, Donald B.; Denney, Dorothy Z.; Liu, Lun-Tsu
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 1 - 8
