3,4-二溴呋喃-2(5H)-酮合成路线 (共 15 条)
反应条件
sodium tetrahydroborate in methanol T=0°C;
参考文献
Cunha, Silvio; Oliveira, Caio C.; Sabino, Jose R.
Journal of the Brazilian Chemical Society, 2011 , vol. 22, # 3 p. 598 - 603
参考文献
American Chemical Journal, , vol. 16, p. 208
Justus Liebigs Annalen der Chemie, , vol. 232, p. 86
Chemische Berichte, , vol. 12, p. 1203
反应条件
carbon disulfide; phosphorus; iodine anschliessend Behandeln mit Wasser;
参考文献
American Chemical Journal, , vol. 16, p. 208
反应条件
water; hydrogen bromide
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 148, p. 420
参考文献
Bulletin de la Societe Chimique de France, , p. 339
反应条件
triphenyl-arsane; tris(dibenzylideneacetone)dipalladium (0) in 1-methyl-pyrrolidin-2-one T=20°C; 89 h;
参考文献
Bellina, Fabio; Anselmi, Chiara; Viel, Stephane; Mannina, Luisa; Rossi, Renzo
Tetrahedron, 2001 , vol. 57, # 50 p. 9997 - 10007
反应条件
dichloro bis(acetonitrile) palladium(II); triphenyl-arsane; silver(l) oxide in tetrahydrofuran T=65°C; Suzuki Coupling; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Pereira, Ulisses A.; Barbosa, Luiz C.A.; Maltha, Celia R.A.; Demuner, Antonio J.; Masood, Mohammed A.; Pimenta, Andrea L.
European Journal of Medicinal Chemistry, 2014 , vol. 82, p. 127 - 138
参考文献
Hill; Cornelison
American Chemical Journal, 1894 , vol. 16, p. 208
反应条件
cesium fluoride; bis-triphenylphosphine-palladium(II) chloride; N-benzyl-N,N,N-triethylammonium chloride in water; toluene T=20 - 25°C; Suzuki Coupling; 72 h;
参考文献
Blazecka, Peter Garth; Zhang, Ji
Patent: US2005/131239 A1, 2005 ;
Location in patent: Page/Page column 8 ;
反应条件
triphenyl-arsane; tris(dibenzylideneacetone)dipalladium (0) in 1-methyl-pyrrolidin-2-one T=20°C; 22 h;
参考文献
Bellina, Fabio; Anselmi, Chiara; Viel, Stephane; Mannina, Luisa; Rossi, Renzo
Tetrahedron, 2001 , vol. 57, # 50 p. 9997 - 10007