1-(3,5-二甲氧基苯基)乙醇合成路线 (共 16 条)
反应条件
in water 2.5 h; Ambient temperatureIrradiationother solvent, (18)O-labeled molecule; MechanismProduct distribution;
参考文献
Jaeger, David A.; Angelos, George H.
Tetrahedron Letters, 1981 , vol. 22, p. 803 - 806
反应条件
jones reagent in acetone 0.5 h; Ambient temperature;
参考文献
Cristol, Stanley J.; Ali, Mahfuza B.; Sankar, Iyer V.
Journal of the American Chemical Society, 1989 , vol. 111, # 21 p. 8207 - 8211
反应条件
1: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature
2: ethanethiol, NaH / dimethylformamide / 3 h / Heating
View Scheme
参考文献
Ayer, William A.; Browne, Lois M.; Lovell, Sarah H.
Phytochemistry (Elsevier), 1983 , vol. 22, # 10 p. 2267 - 2272
反应条件
1: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature
2: NaI, ClSiMe3 / acetonitrile / 36 h / Heating
View Scheme
参考文献
Ayer, William A.; Browne, Lois M.; Lovell, Sarah H.
Phytochemistry (Elsevier), 1983 , vol. 22, # 10 p. 2267 - 2272
反应条件
toluene-4-sulfonic acid in benzene
4 h; Heating;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1480 - 1492
反应条件
sulfuric acid; hydrogen; palladium on activated charcoal in ethyl acetate
P=2942.03 Torr; 4 h; Ambient temperature; Yield given;
参考文献
Ayer, William A.; Browne, Lois M.; Lovell, Sarah H.
Phytochemistry (Elsevier), 1983 , vol. 22, # 10 p. 2267 - 2272