(Z)-7-十二碳烯-1-醇乙酸酯合成路线 （共 65 条）
反应条件
2: 92 percent / pyridine / benzene
View Scheme
参考文献
Basavaiah, D.; Brown, Herbert C.
Journal of Organic Chemistry, 1982 , vol. 47, # 9 p. 1792 - 1793
Title/Abstract Full Text View citing articles Show Details
Brown, Herbert C.; Basavaiah, Deevi; Singh, Shankar M.; Bhat, Narayan G.
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 246 - 250
反应条件
2: 92 percent / pyridine / benzene
View Scheme
参考文献
Basavaiah, D.; Brown, Herbert C.
Journal of Organic Chemistry, 1982 , vol. 47, # 9 p. 1792 - 1793
Title/Abstract Full Text View citing articles Show Details
Brown, Herbert C.; Basavaiah, Deevi; Singh, Shankar M.; Bhat, Narayan G.
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 246 - 250
反应条件
pyridine
3 h; Ambient temperature;
参考文献
Horiike; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 9 p. 2229 - 2230
反应条件
1: 9-BBN; t-BuOK
2: LiAlH4
3: pyridine
View Scheme
参考文献
Bykov; Goletiani; Butenko; Finkel'shtein
Doklady Chemistry, 2002 , vol. 384, # 4-6 p. 163 - 166
反应条件
1: 88 percent / lithium diisopropylamide / tetrahydrofuran / 0.25 h / -78 °C
2: 80 percent / CuBr*S(CH3)2 / tetrahydrofuran / -79 °C
3: acetic acid / 80 °C
View Scheme
参考文献
Macdonald, Timothy L.; Narayanan, Amirthalingam B.; O'Dell, Dale E.
Journal of Organic Chemistry, 1981 , vol. 46, # 7 p. 1504 - 1506
反应条件
1: 80 percent / CuBr*S(CH3)2 / tetrahydrofuran / -79 °C
2: acetic acid / 80 °C
View Scheme
参考文献
Macdonald, Timothy L.; Narayanan, Amirthalingam B.; O'Dell, Dale E.
Journal of Organic Chemistry, 1981 , vol. 46, # 7 p. 1504 - 1506
反应条件
in acetic acid
T=80°C; Yield given. Title compound not separated from byproducts;
参考文献
Macdonald, Timothy L.; Narayanan, Amirthalingam B.; O'Dell, Dale E.
Journal of Organic Chemistry, 1981 , vol. 46, # 7 p. 1504 - 1506
反应条件
1: 80 percent / tetrahydrofuran / 0.5 h / -20 °C
2: 1.) 9-borabicyclo<3.3.1>nonane, 2.) glacial acetic acid / 1.) THF, 0 deg C, 2 h, 2.) THF, 25 deg C, 17 h
View Scheme
参考文献
Tucker; Knochel
Synthesis, 1993 , # 5 p. 530 - 536
反应条件
1: NaOEt / tetrahydrofuran / 1 h / 25 °C
2: n-BuLi / toluene / 2 h / 25 °C
3: lithium aluminium hydride / tetrahydrofuran / 4 h / Heating
4: pyridine / 24 h / 25 °C
View Scheme
参考文献
Vinczer, Peter; Juvancz, Zoltan; Novak, Lajos; Szantay, Csaba
Acta Chimica Hungarica, 1988 , vol. 125, # 6 p. 797 - 820
反应条件
9-borabicyclo[3.3.1]nonane dimer; acetic acid
1) THF, 25 deg C, 3.5h 2) THF, 25 deg C, 2h; Yield given. Multistep reaction;
参考文献
Tucker, Charles E.; Rao, S. Achyutha; Knochel, Paul
Journal of Organic Chemistry, 1990 , vol. 55, # 20 p. 5446 - 5448
