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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
149623-91-6
合成路线
（共 7 条）
149623-91-6
→
反应条件
78842-13-4
2'-氟-2'-脱氧鸟苷
反应条件
1: 23 percent / p-TsOH / 0.83 h / 160 °C / 25 Torr 2: 75 percent / NaN3 / ethanol; H2O / 1.) reflux, 1 h, 2.) room temperature, 20 h 3: 94 percent / H2 / Pd on carbon / ethanol; N,N-dimethyl-acetamide / 20 h / Ambient temperature 4: 79 percent / MeONa / methanol / 1 h / Ambient temperature 5: 83 percent / H2O / 20 h / Ambient temperature; adenosine deaminase View Scheme
参考文献
Thomas; Tiwari; Clayton; Secrist III; Montgomery
Nucleosides and Nucleotides, 1994 , vol. 13, # 1-3 p. 309 - 323
149623-91-6
→
反应条件
78842-13-4
2'-氟-2'-脱氧鸟苷
反应条件
Multistep reaction;
参考文献
Zaitseva, Galina V.; Zinchenko, Anatoli I.; Barai, Vladimir N.; Pavlova; Boreko, Evgeny I.; Mikhailopulo, Igor A.
Nucleosides and Nucleotides, 1999 , vol. 18, # 4-5 p. 687 - 688
149623-91-6
→
反应条件
20187-82-0
反应条件
1: 0.5 g / SnCl4 / acetonitrile; 1,2-dichloro-ethane / Heating 2: methanol. NH3 / 24 h / 20 °C View Scheme
参考文献
Mikhailopulo, Igor A.; Sivets, Grigorii G.; Poopeiko, Nicolai E.; Khripach, Natalia B.
Carbohydrate Research, 1995 , vol. 278, # 1 p. 71 - 90
149623-91-6
→
反应条件
20187-82-0
反应条件
tin(IV) chloride 1.) 1,2-dichloroethane, MeCN, reflux, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mikhailopulo; Sivets; Poopeiko; Khripach
Nucleosides and Nucleotides, 1995 , vol. 14, # 3-5 p. 381 - 382
149623-91-6
→
反应条件
20187-82-0
反应条件
1: 0.5 g / SnCl4 / acetonitrile; 1,2-dichloro-ethane / Heating 2: methanol. NH3 / 24 h / 20 °C View Scheme
参考文献
Mikhailopulo, Igor A.; Sivets, Grigorii G.; Poopeiko, Nicolai E.; Khripach, Natalia B.
Carbohydrate Research, 1995 , vol. 278, # 1 p. 71 - 90
149623-91-6
→
反应条件
20187-82-0
反应条件
tin(IV) chloride 1.) 1,2-dichloroethane, MeCN, reflux, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mikhailopulo; Sivets; Poopeiko; Khripach
Nucleosides and Nucleotides, 1995 , vol. 14, # 3-5 p. 381 - 382
149623-91-6
→
反应条件
134444-47-6
2-氨基-2'-氟-2'-脱氧腺苷
反应条件
1: 23 percent / p-TsOH / 0.83 h / 160 °C / 25 Torr 2: 75 percent / NaN3 / ethanol; H2O / 1.) reflux, 1 h, 2.) room temperature, 20 h 3: 94 percent / H2 / Pd on carbon / ethanol; N,N-dimethyl-acetamide / 20 h / Ambient temperature 4: 79 percent / MeONa / methanol / 1 h / Ambient temperature View Scheme
参考文献
Thomas; Tiwari; Clayton; Secrist III; Montgomery
Nucleosides and Nucleotides, 1994 , vol. 13, # 1-3 p. 309 - 323
