1-(4-{[叔丁基(二甲基)-甲硅烷基]氧基}苯基)乙酮合成路线 （共 9 条）
反应条件
1H-imidazole in N,N-dimethyl-formamide T=20°C; 24 h;
参考文献
Noji, Masahiro; Ohno, Tomoko; Fuji, Koji; Futaba, Noriko; Tajima, Hiroyuki; Ishii, Keitaro
Journal of Organic Chemistry, 2003 , vol. 68, # 24 p. 9340 - 9347
反应条件
in DMF (N,N-dimethyl-formamide) T=20°C; 0.75 h;
参考文献
Boehringer Ingelheim Pharmaceuticals, Inc.
Patent: US2004/102492 A1, 2004 ;
Location in patent: Page 43 ;
反应条件
sodium hypochlorite; sodium hydrogencarbonate; potassium bromide; TEMPO-linked 5,10,15,20-tetraphenyl-Mn-porphyrin in dichloromethane T=0°C; pH=8.6; 0.5 h;
参考文献
Huang, Jian-Ying; Li, Shi-Jun; Wang, Yan-Guang
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5637 - 5640
反应条件
perchloric acid immobilized on silica gel in dichloromethane T=20°C; 0.5 h;
参考文献
Du, Ti-Jian; Wu, Qin-Pei; Liu, Hai-Xia; Chen, Xi; Shu, Yi-Nan; Xi, Xiao-Dong; Zhang, Qing-Shan; Li, Yun-Zheng
Tetrahedron, 2011 , vol. 67, # 6 p. 1096 - 1101
反应条件
Mn-graphite -78 deg C -> RT;
参考文献
Fuerstner, Alois; Brunner, Heiko
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7009 - 7012
反应条件
sodium methylate 1.) DMF, rt, 30 min, 2.) DMF, rt, 1 h; Yield givenMultistep reaction;
参考文献
Oriyama, Takeshi; Noda, Kojiro; Sugawara, Satomi
Synthetic Communications, 1999 , vol. 29, # 13 p. 2217 - 2223
反应条件
cesium fluoride in N,N-dimethyl-formamide 12 h; Ambient temperature;
参考文献
Oriyama, Takeshi; Noda, Kojiro; Yatabe, Kaori
Synlett, 1997 , vol. 1997, # 6 p. 701 - 703
反应条件
water; potassium carbonate in ethanol T=75°C; 16 h;
参考文献
Wilson, Noel S.; Keay, Brian A.
Tetrahedron Letters, 1997 , vol. 38, # 2 p. 187 - 190
反应条件
1: With trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine in dichloromethane T=0°C; 0.5 h; 2: With N-bromosuccinmide in dichloromethane T=20°C; 4 h;
参考文献
Xing, Xuechao; Ho, Pei; Bourquin, Geoffroy; Yeh, Li-An; Cuny, Gregory D.
Tetrahedron, 2003 , vol. 59, # 50 p. 9961 - 9969
