反应条件
in tetrahydrofuran; diethylene glycol dimethyl ether
other Radiation; heating of diglyme and thf soln. of Mo(CO)6 (1 equiv.) and PPh3 (1 equiv.) for 40 min in microwave oven; cooling in ice bath, pptn., filtration, washing with hexane, drying in air; removal of thf and hexane from the washing under reduced pressure, cooling in ice bath, pptn., filtration, washing with cold hexane, drying in air;
参考文献
Ardon, Michael; Hogarth, Graeme; Oscroft, Daniel T.W.
Journal of Organometallic Chemistry, 2004 , vol. 689, # 15 p. 2429 - 2435
