反应条件
in acetonitrile
preparation under dry nitrogen; Mo(CO)6 and TMNO were added to acetonitrle giving a yellow solution; PPh3 was added to the mixture; stirring for 16h at room temperature; filtration; filtrate was cooled at -20°C; recrystallization in CHCl3/EtOH; TA, elem. anal.;
参考文献
Hor, T. S. Andy; Chan, Hardy S. O.; Chiam, Caroline S. M.; Lim, Kok Hwa
Thermochimica Acta, 1988 , vol. 128, p. 175 - 184
