4-溴-3-(2-氯苯基)-1H-吡唑合成路线 （共 2 条）
反应条件
N-bromosuccinmide in dichloromethane T=20°C; 0.833333 h;
参考文献
MILLENNIUM PHARMACEUTICALS, INC.; Chau, Ryan W.; Cullis, Courtney A.; Duffey, Matthew O.; Gipson, Krista E.; Hu, Yongbo; Li, Gang; Sintchak, Michael D.; Vos, Tricia J.
Patent: US2013/165464 A1, 2013 ;
Location in patent: Paragraph 0975 ;
反应条件
1: caesium carbonate; tetrakis (triphenylphosphine) palladium (0) / 1,4-dioxane; water / 0.83 h / 150 °C / |Sealed tube; |Microwave irradiation 2: N-bromosuccinmide / dichloromethane / 0.83 h / 20 °C View Scheme
参考文献
MILLENNIUM PHARMACEUTICALS, INC.; Chau, Ryan W.; Cullis, Courtney A.; Duffey, Matthew O.; Gipson, Krista E.; Hu, Yongbo; Li, Gang; Sintchak, Michael D.; Vos, Tricia J.
Patent: US2013/165464 A1, 2013 ;
