三（2-甲氧基乙氧基）硼酸合成路线 （共 17 条）
反应条件
1: With sodium hydrogencarbonate T=130°C; 21 h; 2: With water 0.5 h; Heating / reflux;
参考文献
Isis Pharmaceuticals Inc.
Patent: US2004/29273 A1, 2004 ;
Location in patent: Page/Page column 18-19 ;
US 20040029273 A1
反应条件
1: With sodium hydrogencarbonate in 2-methoxy-ethanol T=130°C; 21 h; 2: in water T=100°C; 0.5 h;
参考文献
Isis Pharmaceuticals, Inc.
Patent: US2004/14699 A1, 2004 ;
Location in patent: Page/Page column 18 ;
反应条件
in 2-methoxy-ethanol; water T=155 - 160°C; 48 h;
参考文献
Bhanot, Sanjay; Monia, Brett P.; Geary, Richard S.; Kjems, Lise Lund
Patent: US2006/89325 A1, 2006 ;
Location in patent: Page/Page column 14-15 ;
反应条件
in dichloromethane; 2-methoxy-ethanol; acetone; acetonitrile
参考文献
Isis Pharmaceuticals Inc.
Patent: US5958772 A1, 1999 ;
反应条件
T=155 - 160°C; 48 h;
参考文献
Bennett, C. Frank; Dobie, Kenneth W.; Jain, Ravi
Patent: US2005/107324 A1, 2005 ;
Location in patent: Page/Page column 26 ;
反应条件
in pyridine; methanol; dichloromethane; chloroform; 2-methoxy-ethanol; acetone; acetonitrile
参考文献
Isis Pharmaceuticals Inc.
Patent: US5981732 A1, 1999 ;
反应条件
in dichloromethane; acetone; acetonitrile
参考文献
South Alabama Medical Science Foundation; ISIS Pharmaceuticals, Inc.
Patent: US5948902 A1, 1999 ;
