(R)-2-联苯膦,2’-羟基-1,1’-联萘合成路线 （共 10 条）
反应条件
trichlorosilane; triethylamine in toluene T=100°C; 16 h;
参考文献
Uozumi, Yasuhiro; Tanahashi, Asako; Lee, Sang-Yong; Hayashi, Tamio
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1945 - 1948
反应条件
hydrogenchloride in tetrahydrofuran; water
反应条件
1: 91 percent / Nafion-NR50 ion-exchange resin / o-xylene / 16 h / Heating 2: 68 percent / glac. HOAc / 0.17 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 130, # 11 p. 1663 - 1670
反应条件
1: 95 percent / diisopropylethylamine / palladium diacetate, 1,4-bis(diphenylphosphino)butane / dimethylsulfoxide / 12 h / 100 °C 2: 99 percent / 3N aq. NaOH / methanol; dioxane / 12 h / Ambient temperature 3: 94 percent / NEt3, Cl3SiH / toluene / 16 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1945 - 1948
反应条件
1: 95 percent / diisopropylethylamine / palladium diacetate, 1,4-bis(diphenylphosphino)butane / dimethylsulfoxide / 12 h / 100 °C 2: 99 percent / 3N aq. NaOH / methanol; dioxane / 12 h / Ambient temperature 3: 94 percent / NEt3, Cl3SiH / toluene / 16 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1945 - 1948
反应条件
1: 99 percent / 3N aq. NaOH / methanol; dioxane / 12 h / Ambient temperature 2: 94 percent / NEt3, Cl3SiH / toluene / 16 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1945 - 1948
反应条件
acetic acid 0.166667 h; Heating;
参考文献
Kadyrov, Renat; Heinicke, Joachim; Kindermann, Markus K.; Heller, Detlef; Fischer, Christine; Selke, Ruediger; Fischer, Axel K.; Jones, Peter G.
Chemische Berichte, 1997 , vol. 130, # 11 p. 1663 - 1670
反应条件
1: 68 percent / glac. HOAc / 0.17 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 130, # 11 p. 1663 - 1670
反应条件
Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 130, # 11 p. 1663 - 1670
反应条件
camphor-10-sulfonic acid chloride in pyridine
T=100°C; 0.5 h;
参考文献
Kadyrov, Renat; Heinicke, Joachim; Kindermann, Markus K.; Heller, Detlef; Fischer, Christine; Selke, Ruediger; Fischer, Axel K.; Jones, Peter G.
Chemische Berichte, 1997 , vol. 130, # 11 p. 1663 - 1670
