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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
149967-08-8
合成路线
（共 4 条）
501-53-1
氯甲酸苄酯
→
反应条件
149967-08-8
反应条件
1: Na2CO3 / dioxane; H2O / 15 h / 23 °C 2: H2SO4 / CH2Cl2 / 15 h 3: 97 percent / 1N NaOH / methanol / 2 h / 21 °C 4: N-methylmorpholine / tetrahydrofuran / 0.25 h / -10 - 23 °C 5: NaBH4 / tetrahydrofuran; H2O / 3 h / 21 °C View Scheme
参考文献
Brown; Bickett; Chambers; Davies; Deaton; Drewry; Foley; McElroy; Gregson; McGeehan; Myers; Norton; Salovich; Schoenen; Ward
Journal of Medicinal Chemistry, 1994 , vol. 37, # 5 p. 674 - 688
28862-78-4
→
反应条件
149967-08-8
反应条件
1: H2SO4 / CH2Cl2 / 15 h 2: 97 percent / 1N NaOH / methanol / 2 h / 21 °C 3: N-methylmorpholine / tetrahydrofuran / 0.25 h / -10 - 23 °C 4: NaBH4 / tetrahydrofuran; H2O / 3 h / 21 °C View Scheme
参考文献
Brown; Bickett; Chambers; Davies; Deaton; Drewry; Foley; McElroy; Gregson; McGeehan; Myers; Norton; Salovich; Schoenen; Ward
Journal of Medicinal Chemistry, 1994 , vol. 37, # 5 p. 674 - 688
149967-07-7
→
反应条件
149967-08-8
反应条件
1: N-methylmorpholine / tetrahydrofuran / 0.25 h / -10 - 23 °C 2: NaBH4 / tetrahydrofuran; H2O / 3 h / 21 °C View Scheme
参考文献
Brown; Bickett; Chambers; Davies; Deaton; Drewry; Foley; McElroy; Gregson; McGeehan; Myers; Norton; Salovich; Schoenen; Ward
Journal of Medicinal Chemistry, 1994 , vol. 37, # 5 p. 674 - 688
149967-06-6
→
反应条件
149967-08-8
反应条件
1: 97 percent / 1N NaOH / methanol / 2 h / 21 °C 2: N-methylmorpholine / tetrahydrofuran / 0.25 h / -10 - 23 °C 3: NaBH4 / tetrahydrofuran; H2O / 3 h / 21 °C View Scheme
参考文献
Brown; Bickett; Chambers; Davies; Deaton; Drewry; Foley; McElroy; Gregson; McGeehan; Myers; Norton; Salovich; Schoenen; Ward
Journal of Medicinal Chemistry, 1994 , vol. 37, # 5 p. 674 - 688
