[2,2:6,2]四吡啶-6,6-二羧酸合成路线 （共 3 条）
反应条件
potassium hydroxide in methanol T=75°C; 10 h;
参考文献
Petitjean, Anne; Khoury, Richard G.; Kyritsakas, Nathalie; Lehn, Jean-Marie
Journal of the American Chemical Society, 2004 , vol. 126, # 21 p. 6637 - 6647
反应条件
1: 46 percent / tetrakistriphenylphosphinepalladium(0) / toluene / 16 h / Heating 2: 98 percent / aq. KOH / methanol / 10 h / 75 °C View Scheme
参考文献
Petitjean, Anne; Khoury, Richard G.; Kyritsakas, Nathalie; Lehn, Jean-Marie
Journal of the American Chemical Society, 2004 , vol. 126, # 21 p. 6637 - 6647
反应条件
1.1: 3-ClC6H4CO3H / CH2Cl2 / 12 h / 20 °C 2.1: 92 percent / PhCOCl / CH2Cl2 / 12 h / 20 °C 3.1: KOH / ethanol; H2O / Heating 3.2: 92 percent / H2SO4; CH3COOH / 5 h / Heating View Scheme
参考文献
Galaup, Chantal; Couchet, Jean-Marc; Bedel, Sebastien; Tisnes, Pierre; Picard, Claude
Journal of Organic Chemistry, 2005 , vol. 70, # 6 p. 2274 - 2284
