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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-甲氧基苯酚
合成路线
(共 563 条)
150-19-6
3-甲氧基苯酚
+
1449510-54-6
→
反应条件
1655-68-1
3-苯氧基苯甲醚
反应条件
1: 3-methoxy-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: 2,4-dimethoxyphenyl(phenyl)iodonium triflate in tetrahydrofuran T=40°C; chemoselective reaction;
参考文献
Malmgren, Joel; Santoro, Stefano; Jalalian, Nazli; Himo, Fahmi; Olofsson, Berit
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10334 - 10342
150-19-6
3-甲氧基苯酚
+
1449510-56-8
→
反应条件
1655-68-1
3-苯氧基苯甲醚
反应条件
1: 3-methoxy-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: 2,5-dimethoxyphenyl(phenyl)iodonium triflate in tetrahydrofuran T=40°C; Mechanism; chemoselective reaction;
参考文献
Malmgren, Joel; Santoro, Stefano; Jalalian, Nazli; Himo, Fahmi; Olofsson, Berit
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10334 - 10342
150-19-6
3-甲氧基苯酚
+
120976-84-3
→
反应条件
1655-68-1
3-苯氧基苯甲醚
+
58005-59-7
反应条件
1: 3-methoxy-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: phenyl(p-tolyl)iodonium trifluoromethanesulfonate in tetrahydrofuran T=40°C; Overall yield = 78 percent; chemoselective reaction;
参考文献
Malmgren, Joel; Santoro, Stefano; Jalalian, Nazli; Himo, Fahmi; Olofsson, Berit
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10334 - 10342
150-19-6
3-甲氧基苯酚
→
反应条件
1655-68-1
3-苯氧基苯甲醚
+
23951-29-3
反应条件
1: 3-methoxy-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: (2-methylphenyl)(phenyl)iodonium triflate in tetrahydrofuran T=40°C; Overall yield = 98 percent; chemoselective reaction;
参考文献
Malmgren, Joel; Santoro, Stefano; Jalalian, Nazli; Himo, Fahmi; Olofsson, Berit
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10334 - 10342
150-19-6
3-甲氧基苯酚
+
144930-49-4
→
反应条件
479091-12-8
+
1655-68-1
3-苯氧基苯甲醚
反应条件
1: 3-methoxy-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: (2,5-dimethylphenyl)(phenyl)iodonium triflate in tetrahydrofuran T=40°C; Overall yield = > 99 percent; chemoselective reaction;
参考文献
Malmgren, Joel; Santoro, Stefano; Jalalian, Nazli; Himo, Fahmi; Olofsson, Berit
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10334 - 10342
150-19-6
3-甲氧基苯酚
+
1449510-53-5
→
反应条件
反应条件
1: 3-methoxy-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: 2,6-dimethylphenyl(phenyl)iodonium triflate in tetrahydrofuran T=40°C; Overall yield = 98 percent; chemoselective reaction;
参考文献
Malmgren, Joel; Santoro, Stefano; Jalalian, Nazli; Himo, Fahmi; Olofsson, Berit
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10334 - 10342
150-19-6
3-甲氧基苯酚
+
144930-50-7
均三甲苯基(苯基)碘鎓三氟甲磺酸盐
→
反应条件
反应条件
1: 3-methoxy-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: [Ph-I-Mes][OTf] in tetrahydrofuran T=40°C; Overall yield = 84 percent; chemoselective reaction;
参考文献
Malmgren, Joel; Santoro, Stefano; Jalalian, Nazli; Himo, Fahmi; Olofsson, Berit
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10334 - 10342
150-19-6
3-甲氧基苯酚
+
1449510-52-4
→
反应条件
反应条件
1: 3-methoxy-phenol With potassium tert-butylate in tetrahydrofuran T=0°C; 0.25 h; 2: 2,4-dimethylphenyl(phenyl)iodonium triflate in tetrahydrofuran T=40°C; Overall yield = 98 percent; chemoselective reaction;
参考文献
Malmgren, Joel; Santoro, Stefano; Jalalian, Nazli; Himo, Fahmi; Olofsson, Berit
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10334 - 10342
150-19-6
3-甲氧基苯酚
+
107-14-2
氯乙腈
→
反应条件
15832-09-4
6-甲氧基-3-苯并呋喃酮
反应条件
hydrogenchloride; sodium hydroxide; Zinc chloride in 1,4-dioxane; water
参考文献
Phytera, Inc.
Patent: US6307070 B1, 2001 ;
150-19-6
3-甲氧基苯酚
+
107-16-4
+
78-97-7
→
反应条件
15832-09-4
6-甲氧基-3-苯并呋喃酮
反应条件
暂无反应条件数据
参考文献
Slater; Stephen
Journal of the Chemical Society, 1920 , vol. 117, p. 314
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