Van Overschelde, Michel; Vervecken, Elias; Modha, Sachin G.; Cogen, Simon; Van der Eycken, Erik; Van der Eycken, Johan
Tetrahedron, 2009 , vol. 65, # 32 p. 6410 - 6415
in ethanol; chloroform byproducts: H2; Irradiation (UV/VIS); standard inert atmosphere; react. in water-cooled quartz immersion-well photochemical reactor, the borane dissolved in ethanol/chloroform 1-2percent (vol./vol.), irradiation at room temp., 3 h; not isolated, reaction followed by (11)B NMR;
in tetrahydrofuran; toluene THF soln. of B compd. added dropwise to toluene soln. of Zr compd. stirred for 1 h at room temp. and for 30 h at 60°C; NMR;
参考文献
European Journal of Inorganic Chemistry, , # 36 p. 5548 - 5557
