1,4-二叠氮双环[2.2.2]辛烷合成路线 (共 45 条)
参考文献
Bischoff; Nastvogel
Chemische Berichte, 1889 , vol. 22, p. 1784
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile
0.25 h; Ambient temperature;
参考文献
Eynde, Jean Jacques Vanden; Mayence, Annie; Lor, Pascal; Haverbeke, Yves Van
Bulletin des Societes Chimiques Belges, 1995 , vol. 104, # 6 p. 387 - 392
反应条件
methanol; nickel; acetic acid
T=20°C; P=80905.8 Torr; Hydrogenation;
参考文献
Plieninger; Werst
Chemische Berichte, 1955 , vol. 88, p. 1956,1960
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile
6 h; Ambient temperature;
参考文献
Eynde, Jean Jacques Vanden; Delfosse, Florence; Lor, Pascal; Haverbeke, Yves Van
Tetrahedron, 1995 , vol. 51, # 20 p. 5813 - 5818
反应条件
(i) ClCO2Et, Et3N, (ii) /BRN= 646740/; Multistep reaction;
参考文献
Bayer AG
Patent: DE2515146 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 71947