2-甲酰基-5-(甲氧基甲基)噻吩合成路线 （共 17 条）
反应条件
1.1: sodium hydride / hexane; tetrahydrofuran / 0.5 h / 20 °C 1.2: 16 h / 20 °C 2.1: n-butyllithium / hexane; tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide / 0.03 h / -78 °C 2.2: 20 °C View Scheme
参考文献
RUTGERS, THE STATE UNIVERSITY OF NEW JERSEY; PROVID PHARMACEUTICALS INC.; EBRIGHT, Richard H.; EBRIGHT, Yon W.; SHEN, Juan; BACCI, James; HIEBEL, Anne-Cecile; SOLVIBILE, William; SELF, Christopher; OLSON, Gary
Patent: WO2013/192352 A1, 2013 ;
反应条件
1: silver carbonate 2: hydrogen bromide 3: silver carbonate / 48 h View Scheme
参考文献
Nam Shin, Jeong E.; Perlin, Arthur S.
Carbohydrate Research, 1980 , vol. 84, p. 315 - 327
反应条件
1: hydrogen bromide 2: silver carbonate / 48 h View Scheme
参考文献
Nam Shin, Jeong E.; Perlin, Arthur S.
Carbohydrate Research, 1980 , vol. 84, p. 315 - 327
反应条件
silver carbonate 48 h;
参考文献
Nam Shin, Jeong E.; Perlin, Arthur S.
Carbohydrate Research, 1980 , vol. 84, p. 315 - 327
反应条件
hydrogenchloride; water in methanol 34 h; Heating;
参考文献
Hashimoto, Hironobu; Yuasa, Hideya
Tetrahedron Letters, 1988 , vol. 29, # 16 p. 1939 - 1942
参考文献
Nam Shin, Jeong E.; Perlin, Arthur S.
Carbohydrate Research, 1980 , vol. 84, p. 315 - 327
反应条件
in water 13 h; Heating2.8percent HCl; other concn.; other 5-thio-D-glucose derivatives; Product distribution;
参考文献
Yuasa, Hideya; Tamura, Jun-ichi; Hashimoto, Hironobu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 10 p. 2763 - 2769
