4-(羟基亚氨基)哌啶-1-羧酸叔丁酯合成路线 (共 7 条)
反应条件
hydroxylamine hydrochloride; sodium acetate in ethanol; water
参考文献
Mullen, Philip; Miel, Hugues; Anthony McKervey
Tetrahedron Letters, 2010 , vol. 51, # 24 p. 3216 - 3217
反应条件
hydroxylamine hydrochloride in methanol
参考文献
SmithKline Beecham Corporation
Patent: US6077857 A1, 2000 ;
反应条件
triethylamine in methanol; chloroform; hydroxylamine hydrochloride
反应条件
hydrogen; Raney nickel in ethanol P=2585.81 Torr;
参考文献
SCHERING CORPORATION
Patent: EP937069 B1, 2006 ;
Location in patent: Page/Page column 46-47 ;
反应条件
1-propanephosphonic acid cyclic anhydride in tetrahydrofuran; ethyl acetate T=70°C; Beckmann rearrangement; Inert atmosphere;
参考文献
Augustine, John Kallikat; Kumar, Rajesha; Bombrun, Agnes; Mandal, Ashis Baran
Tetrahedron Letters, 2011 , vol. 52, # 10 p. 1074 - 1077
反应条件
1: With triethylamine in acetonitrile T=20°C; 0.5 h; 2: in water; acetonitrile T=20°C;
参考文献
TEIJIN LIMITED
Patent: EP1477490 A1, 2004 ;
Location in patent: Page 109 ;
EP 1477490 A1
反应条件
dihydrogen peroxide; sodium hydrogencarbonate; urea; trifluoroacetic anhydride in water; acetonitrile 4 h; Reflux;
参考文献
Mullen, Philip; Miel, Hugues; Anthony McKervey
Tetrahedron Letters, 2010 , vol. 51, # 24 p. 3216 - 3217