1-甲基吲哚-3-乙酰胺合成路线 （共 10 条）
反应条件
sodium hydroxide; tetrabutylammomium bromide; dihydrogen peroxide in dichloromethane; water T=0 - 20°C; Hydrolysis;
参考文献
Faul, Margaret M.; Winneroski, Leonard L.; Krumrich, Christine A.
Journal of Organic Chemistry, 1998 , vol. 63, # 17 p. 6053 - 6058
反应条件
hydrogenchloride; sodium hydroxide; tetrabutylammomium bromide; dihydrogen peroxide in dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide
反应条件
hydrogenchloride; sodium hydroxide; tetrabutylammomium bromide; dihydrogen peroxide in dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide
反应条件
pyridine; NH4(HCO3); di-tert-butyl dicarbonate in 1,4-dioxane 18 h;
参考文献
Zhu, Shaolin; MacMillan, David W. C.
Journal of the American Chemical Society, 2012 , vol. 134, # 26 p. 10815 - 10818
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
Neel, David A.; Jirousek, Michael R.; McDonald III, John H.
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 1 p. 47 - 50
反应条件
1: 100 percent / NaH / dimethylformamide / 3 h / 0 - 20 °C 2: 70 percent / tetrabutylammonium bromide; hydrogen peroxide; NaOH / CH2Cl2; H2O / 0 - 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 17 p. 6053 - 6058
反应条件
1,4-dioxane; ammonium polysulfide T=170°C;
参考文献
Sb. Statei Obshch. Khim., , p. 712
Chem.Abstr., , p. 1006
参考文献
Journal of the Chemical Society, , p. 2586,2591
参考文献
Baskakow; Mel'nikow
Sb. Statei Obshch. Khim., 1953 , p. 712
Chem.Abstr., 1955 , p. 1006
反应条件
potassium tert-butylate in tetrahydrofuran T=-5 - 45°C;
参考文献
Faul, Margaret M.; Grutsch, John L.; Kobierski, Michael E.; Kopach, Michael E.; Krumrich, Christine A.; Staszak, Michael A.; Udodong, Uko; Vicenzi, Jeffrey T.; Sullivan, Kevin A.
Tetrahedron, 2003 , vol. 59, # 36 p. 7215 - 7229
