3,4,5-三甲氧基苯基乙二醛水合物合成路线 (共 4 条)
反应条件
selenium(IV) oxide in 1,4-dioxane
参考文献
El-Mahdy, Ahmed F. M.; Shibata, Takayuki; Kabashima, Tsutomu; Kai, Masaaki
Chemical Communications, 2014 , vol. 50, # 7 p. 859 - 861
反应条件
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 19 h / 20 °C 2: dimethyl sulfoxide / 60 h / 40 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 7 p. 1439 - 1447
反应条件
dimethyl sulfoxide T=40°C; 60 h;
参考文献
European Journal of Organic Chemistry, , # 7 p. 1439 - 1447
反应条件
1: isopropylmagnesium chloride / tetrahydrofuran / -78 - 0 °C / Inert atmosphere 2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 19 h / 20 °C 3: dimethyl sulfoxide / 60 h / 40 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 7 p. 1439 - 1447