4,4’-二羟基二苯二硫醚合成路线 (共 21 条)
反应条件
N-phenyltriazolinedione in toluene T=20°C; 0.166667 h;
参考文献
Christoforou, Angelos; Nicolaou, Georgia; Elemes, Yiannis
Tetrahedron Letters, 2006 , vol. 47, # 52 p. 9211 - 9213
反应条件
NaY faujasite T=150°C; 13 h;
参考文献
Selva, Maurizio; Tundo, Pietro
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1464 - 1470
反应条件
in dimethyl sulfoxide
反应条件
hydrogenchloride in pyridine T=220°C; 0.166667 h;
参考文献
LaLonde, Robert T.; Eckert, Timothy S.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2298 - 2302
反应条件
sulfur; copper(l) iodide; sodium acetate in N,N-dimethyl-formamide T=100°C; 168 h; Inert atmosphere;
参考文献
Organometallics, , vol. 32, # 19 p. 5514 - 5522
反应条件
sulfur; copper(l) iodide; lithium hydroxide hydrate in N,N-dimethyl-formamide T=100°C; 168 h; Inert atmosphere;
参考文献
Organometallics, , vol. 32, # 19 p. 5514 - 5522
反应条件
1: (i) SOCl2, DMF, (ii) Zn, H2SO4 2: I2, NaOH / aq. ethanol View Scheme
参考文献
Tetrahedron, , vol. 25, p. 4583 - 4591
反应条件
air in water 3 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, , vol. 17, # 10 p. 2161 - 2170
反应条件
1: 2-methyl-propan-2-ol; H2O / 3 h / 20 - 25 °C / Irradiation; DRL-400 mercury lamp (400 W) 2: KOH / H2O / 0.33 h / Heating 3: air / H2O / 3 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, , vol. 17, # 10 p. 2161 - 2170
反应条件
sodium hydroxide; Na2S2 T=90°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 3214
J. Gen. Chem. USSR (Engl. Transl.), , vol. 27, p. 3251