4-(三氟甲氧基)苯甲醛肟合成路线 (共 4 条)
反应条件
hydroxylamine hydrochloride; sodium carbonate in ethanol; water T=60°C; 1 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 12, # 15 p. 3965 - 3970
反应条件
toluene-4-sulfonic acid; 1,2-bis-(diphenylphosphino)ethane; carbonyl(dihydro)tris(triphenylphosphine)ruthenium(II) in toluene Heating;
参考文献
Owston, Nathan A.; Parker, Alexandra J.; Williams, Jonathan M. J.
Organic Letters, 2007 , vol. 9, # 18 p. 3599 - 3601
反应条件
1,1,3,3-tetraphenyl-2-oxa-1,3-phoshpinobenzene bis(trifluoromethanesulfonate); triethylamine in dichloromethane T=20°C; 0.333333 h;
参考文献
Moussa, Ziad
Synthesis, 2012 , vol. 44, # 3 art. no. T105811SS, p. 460 - 468
反应条件
hydrogenchloride; hydrogen; palladium 10 on activated carbon in ethanol; water
P=760.051 Torr;
参考文献
INSTITUTE OF MATERIA MEDICA, CHINESE ACADEMY OF MEDICAL SCIENCES
Patent: EP2511283 A1, 2012 ;
Location in patent: Page/Page column 43 ;