3,5-二-叔丁基水杨酸甲酯合成路线 （共 3 条）
反应条件
sulfuric acid in methanol T=20°C; 5 h;
参考文献
Jimenez, Claudio A.; Belmar, Julio B.
Synthetic Communications, 2007 , vol. 37, # 14 p. 2391 - 2397
反应条件
in methanol; water 5 h; Heating;
参考文献
Scheurer, Andreas; Mosset, Paul; Bauer, Walter; Saalfrank, Rolf W.
European Journal of Organic Chemistry, 2001 , # 16 p. 3067 - 3074
反应条件
1.1: 75 percent / aq. KOH / methanol / 4 h / Heating
2.1: DMF / SOCl2 / 12 h / 20 °C
2.2: 93 percent / dimethylaminopyridine / pyridine; H2O / 20 °C
3.1: 92 percent / tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Jimenez, Claudio A.; Belmar, Julio B.
Synthetic Communications, 2007 , vol. 37, # 14 p. 2391 - 2397
