(S)-(+)-2-苯甘氨酸甲酯 盐酸盐合成路线 (共 38 条)
反应条件
thionyl chloride 10 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 55, # 11 p. 3475 - 3483
反应条件
hydrogenchloride; hydrogen; palladium dihydroxide in methanol P=760.051 Torr; 15 h;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 10 p. 1907 - 1909
反应条件
hydrogenchloride T=20°C; 18 h;
参考文献
Tetrahedron, , vol. 57, # 13 p. 2589 - 2595
反应条件
NaPF6; 1,3,5-Tris{[(S,S)-4,5-diphenyl-2-oxazolinyl]methyl}-2,4,6-triethylbenzene in water-d2; chloroform-d1 T=25°C; Resolution of racemate; optical yield given as percent ee;
参考文献
Bulletin of the Korean Chemical Society, , vol. 31, # 3 p. 724 - 726
参考文献
Tetrahedron Letters, , vol. 45, # 52 p. 9565 - 9567
反应条件
(−)-O,O′-di-pivaloyl-L-tartaric acid; lithium diisopropyl amide in tetrahydrofuran; diethyl ether T=-105°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 44, # 17 p. 5495 - 5506
反应条件
thionyl chloride 20 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 11 p. 1853 - 1856
反应条件
1: Na2SO4 / methanol / 24 h / 20 °C 2: LiClO4 / acetonitrile / 20 °C 3: 91 percent / ceric ammonium nitrate / acetonitrile; H2O / 4 h / 20 °C 4: 88 percent / HCl View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 52 p. 9565 - 9567
反应条件
1: LiClO4 / acetonitrile / 20 °C 2: 91 percent / ceric ammonium nitrate / acetonitrile; H2O / 4 h / 20 °C 3: 88 percent / HCl View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 52 p. 9565 - 9567
反应条件
1: 91 percent / ceric ammonium nitrate / acetonitrile; H2O / 4 h / 20 °C 2: 88 percent / HCl View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 52 p. 9565 - 9567