反应条件
1: 1-bromo-4-methoxy-benzene With tert.-butyl lithium in tetrahydrofuran; pentane
T=-78 - 20°C; Inert atmosphere;
2: With zinc(II) chloride in tetrahydrofuran; pentane
T=0 - 20°C; Inert atmosphere;
3: 2-naphthyl 2,2,2-trimethylacetate With Ni(PCy3)2Cl2 in tetrahydrofuran; N,N-dimethyl acetamide; pentane
T=70°C; 3 h; Inert atmosphere;
参考文献
Li, Bi-Jie; Li, Yi-Zhou; Lu, Xing-Yu; Liu, Jia; Guan, Bing-Tao; Shi, Zhang-Jie
Angewandte Chemie - International Edition, 2008 , vol. 47, # 52 p. 10124 - 10127