2-(3-吡啶基)-2-丙醇合成路线 (共 18 条)
反应条件
methyllithium in tetrahydrofuran; diethyl ether
参考文献
British Technology Group Limited
Patent: US5595995 A1, 1997 ;
反应条件
in diethyl ether; benzene T=25°C; 1.5 h; ketone/MeLi ratio 1:2;
参考文献
Epsztajn, Jan; Bieniek, Adam
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 213 - 220
反应条件
1: ethylmagnesium bromide; methyllithium in tetrahydrofuran; diethyl ether T=-78°C; 1 h; 2: 3-acetyl-pyridine in tetrahydrofuran; diethyl ether T=-78°C; 1 h;
参考文献
Hatano, Manabu; Matsumura, Tokihiko; Ishihara, Kazuaki
Organic Letters, 2005 , vol. 7, # 4 p. 573 - 576
反应条件
methyl-magnesium iodide; diethyl ether
参考文献
Bachman; Micucci
Journal of the American Chemical Society, 1948 , vol. 70, p. 2381,2383
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Graf
Journal fuer Praktische Chemie (Leipzig), 1936 , vol. <2> 146, p. 88,102
反应条件
methyl-magnesium iodide; diethyl ether
参考文献
Brown; Murphey
Journal of the American Chemical Society, 1951 , vol. 73, p. 3308,3310
参考文献
Hartsel, Joshua A.; Craft, Derek T.; Chen, Qiao-Hong; Ma, Ming; Carlier, Paul R.
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3127 - 3133
参考文献
Oparina
Monatshefte fuer Chemie, 1931 , vol. 57, p. 335
Chem. Zentralbl., 1926 , vol. 97, # I p. 3336
反应条件
magnesium 1.) ether, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Robinson, Derek I.; Sherrington David C.; Suckling, Colin J.
Journal of Chemical Research, Miniprint, 1985 , # 5 p. 1701 - 1728
反应条件
in methanol 6 h; Irradiation;
参考文献
Fasani, Elisa; Mella, Mariella; Monti, Sandra; Sortino, Salvatore; Albini, Angelo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 9 p. 1889 - 1894
反应条件
lauryl mercaptan in cyclohexane Irradiation; Quantum yieldProduct distribution;
参考文献
Fasani, Elisa; Mella, Mariella; Monti, Sandra; Sortino, Salvatore; Albini, Angelo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 9 p. 1889 - 1894