5,7-二甲基-3,4-二氢-1H-2-萘酮合成路线 （共 4 条）
反应条件
titanium tetrachloride in dichloromethane T=0 - 20°C; Friedel Crafts reaction; 2.5 h;
参考文献
Hon, Yung-Son; Devulapally, Rammohan
Tetrahedron Letters, 2009 , vol. 50, # 41 p. 5713 - 5715
反应条件
1: NaBH4, CH3OH / toluene / 0 °C 2: 20percent aq. (COOH)2 / 5 h / Heating 3: 30percent H2O2 / 0.75 h / 30 - 35 °C 4: 20percent H2SO4 / 4 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 16 p. 2279 - 2291
反应条件
1: 30percent H2O2 / 0.75 h / 30 - 35 °C 2: 20percent H2SO4 / 4 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 16 p. 2279 - 2291
反应条件
1: 20percent aq. (COOH)2 / 5 h / Heating 2: 30percent H2O2 / 0.75 h / 30 - 35 °C 3: 20percent H2SO4 / 4 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 16 p. 2279 - 2291
