反应条件
in diethyl ether N2 atmosphere; stirring (14 h, room temp.); removal of solvent (vac.), dissoln. (CH2Cl2/petroleum ether 1:5), chromy. (CH2Cl2/petroleum ether 1:5 and 4:1), concn. (vac.), cooling (-78°C); elem. anal.;
参考文献
Dossett, Stephen J.; Hill, Anthony F.; Howard, Judith A. K.; Nasir, Bashir A.; Spaniol, Thomas P.; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1871 - 1878