反应条件
1: sodium hydride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / |Inert atmosphere 2: diisobutylaluminium hydride / toluene / 20 °C / |Inert atmosphere 3: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 - 20 °C / |Inert atmosphere 4: palladium 10 on activated carbon; hydrogen / methanol / 3 h / 20 °C 5: 1,1-dimethylnitroethane; trimethylsilylazide / acetonitrile / 2 h / 20 °C / |Inert atmosphere; |Cooling 6: FeBr2 / toluene / 16 h / 140 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 2 p. 620 - 623
