3-(3,4,5-三甲氧基苯基)-2-丙烯-1-醇合成路线 （共 16 条）
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran Ambient temperature;
参考文献
Ponpipom, Mitree M.; Bugianesi, Robert L.; Brooker, David R.; Yue, Bao-Zhen; Hwang, San-Bao; Shen, Tsung-Ying
Journal of Medicinal Chemistry, 1987 , vol. 30, # 1 p. 136 - 142
反应条件
BaMnO4 in dichloromethane 4 h; Ambient temperature;
参考文献
Banwell, Martin G.; Lambert, John N.; Gravatt, G. Lance
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 22 p. 2817 - 2830
反应条件
[Ir(μ-Cl)(cyclooctene)2]2; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; lithium chloride in water; 1,3,5-trimethyl-benzene T=170°C; 16 h; Schlenk techniqueInert atmosphere; Overall yield = 95percent; Overall yield = 187 mg;
参考文献
Olsen, Esben P. K.; Madsen, Robert
Chemistry - A European Journal, 2012 , vol. 18, # 50 p. 16023 - 16029
反应条件
lithium aluminium tetrahydride in pyridine
2 h; Ambient temperature;
参考文献
Ehret, Charles; Maupetit, Pierre
Phytochemistry (Elsevier), 1982 , vol. 21, # 12 p. 2984 - 2985
反应条件
[Ir(μ-Cl)(cyclooctene)2]2; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; lithium chloride in water; 1,3,5-trimethyl-benzene
T=170°C; 16 h; Schlenk techniqueInert atmosphere; Overall yield = 95percent; Overall yield = 187 mg;
参考文献
Olsen, Esben P. K.; Madsen, Robert
Chemistry - A European Journal, 2012 , vol. 18, # 50 p. 16023 - 16029
反应条件
sodium tetrahydroborate; hydrogen; nickel diacetate in ethanol
参考文献
Bourdron, Julien; Commeiras, Laurent; Barbier, Pascale; Bourgarel-Rey, Veronique; Pasquier, Eddy; Vanthuyne, Nicolas; Hubaud, Jean-Claude; Peyrot, Vincent; Parrain, Jean-Luc
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 16 p. 5540 - 5548
