3-苯基-2-丙炔-1-醇合成路线 (共 165 条)
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine T=20°C; Sonogashira coupling; 5 h; Inert atmosphere;
参考文献
Panteleev, Jane; Huang, Richard Y.; Lui, Erica K. J.; Lautens, Mark
Organic Letters, 2011 , vol. 13, # 19 p. 5314 - 5317
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=-78 - 20°C; 2 h;
参考文献
Braverman, Samuel; Pechenick-Azizi, Tatiana; Gottlieb, Hugo E.; Sprecher, Milon
Synthesis, 2011 , # 11 p. 1741 - 1750
反应条件
pyrrolidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in water T=70°C; 0.5 h;
参考文献
In, Su Kim; Guang, Ri Dong; Young, Hoon Jung
Journal of Organic Chemistry, 2007 , vol. 72, # 14 p. 5424 - 5426
反应条件
piperidine; tetrabutylammomium bromide in water T=60°C; Sonogashira coupling; 5 h;
参考文献
Jin, Myung-Jong; Lee, Dong-Hwan
Angewandte Chemie - International Edition, 2010 , vol. 49, # 6 p. 1119 - 1122
反应条件
trichlorosilane; N,N-dimethyl-formamide in dichloromethane T=0°C; 6 h;
参考文献
Kobayashi, Shu; Yasuda, Masaru; Hachiya, Iwao
Chemistry Letters, 1996 , # 5 p. 407 - 408
反应条件
sodium hydrogencarbonate; palladium diacetate in water; acetonitrile 0.0833333 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Lee, Hong-Woo; Jang, Su-Bum; Ho, Pil-Su
Chemical Communications, 1996 , # 7 p. 835 - 836
反应条件
sodium hydrogencarbonate; palladium diacetate in water; acetonitrile 0.333333 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Lee, Hong-Woo; Jang, Su-Bum; Ho, Pil-Su
Chemical Communications, 1996 , # 7 p. 835 - 836
反应条件
sodium hydrogencarbonate; palladium diacetate in water; acetonitrile 0.333333 h; Ambient temperature;
参考文献
Kang, Suk-Ku; Lee, Hong-Woo; Jang, Su-Bum; Ho, Pil-Su
Chemical Communications, 1996 , # 7 p. 835 - 836
反应条件
potassium carbonate; palladium nanoclusters in methanol; acetonitrile T=20°C; Sonogashira coupling reaction; 4 h;
参考文献
Athilakshmi; Ramanathan; Chand, Dillip Kumar
Tetrahedron Letters, 2008 , vol. 49, # 36 p. 5286 - 5288
反应条件
copper(l) iodide; sodium methylate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in methanol; acetonitrile T=20°C;
参考文献
Kang; Ryu; Lee
Synthetic Communications, 2001 , vol. 31, # 7 p. 1059 - 1064