3-苯基-2-丙炔-1-醇合成路线 （共 165 条）
反应条件
1: Dess-Martin periodane / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
2: trichloroacetic acid sodium salt / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere
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参考文献
Gupta, Manoj K.; Li, Zhexi; Snowden, Timothy S.
Journal of Organic Chemistry, 2012 , vol. 77, # 10 p. 4854 - 4860
反应条件
potassium hydride in tetrahydrofuran
T=0 - 20°C; Inert atmosphere;
参考文献
Corkum, Elizabeth G.; Hass, Michael J.; Sullivan, Andrew D.; Bergens, Steven H.
Organic Letters, 2011 , vol. 13, # 13 p. 3522 - 3525
反应条件
1.1: 58 percent / PBr3; pyridine / diethyl ether / 4 h / 0 °C
2.1: NaH / tetrahydrofuran / 0 °C
2.2: 47 percent / tetrahydrofuran / 1 h / 0 °C
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参考文献
Hashmi, A. Stephen K.; Haufe, Patrick; Rivas Nass, Andreas
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 11 p. 1237 - 1241
参考文献
Fugitt; Wu; Martinelli
Journal of Pharmaceutical Sciences, 1973 , vol. 62, # 11 p. 1894 - 1896
反应条件
1: 65 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 24 h / 20 °C
2: 57 percent / PtCl4 / dioxane / 0.08 h / 20 °C
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参考文献
Pastine, Stefan J.; Youn, So Won; Sames, Dalibor
Organic Letters, 2003 , vol. 5, # 7 p. 1055 - 1058
