(2E)-3-(2-甲氧基苯基)-2-丙烯-1-醇合成路线 （共 14 条）
反应条件
sodium formate; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide; [{(η5-C5Me5)IrCl}2(μ-Cl)2] T=80°C; 0.4 h;
参考文献
Wu, Xiaofeng; Liu, Jianke; Li, Xiaohong; Zanotti-Gerosa, Antonio; Hancock, Fred; Vinci, Daniele; Ruan, Jiwu; Xiao, Jianliang
Angewandte Chemie - International Edition, 2006 , vol. 45, # 40 p. 6718 - 6722
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 0.5 h;
参考文献
Jiang, Tao; Livinghouse, Tom; Lovick, Helena M.
Chemical Communications, 2011 , vol. 47, # 48 p. 12861 - 12863
反应条件
1: With chloroformic acid ethyl ester; triethylamine in tetrahydrofuran T=-7°C; Inert atmosphere; 2: With sodium tetrahydroborate in tetrahydrofuran; methanol T=-7 - 0°C; 16.6667 h;
参考文献
Loelsberg, Wibke; Ye, Shute; Schmalz, Hans-Guenther
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 11-12 p. 2023 - 2031
反应条件
1: 89 percent / diethyl ether; tetrahydrofuran / 0 °C 2: O3ReOSiPh3 / diethyl ether / 0.5 h / -50 °C View Scheme
参考文献
Molina, Pedro; Pastor, Aurelia; Vilaplana, Maria Jesus
Tetrahedron Letters, 1993 , vol. 34, # 23 p. 3773 - 3776
反应条件
diisobutylaluminium hydride Yield given;
参考文献
Kim, Eunha; Koh, Minseob; Lim, Byung Joon; Park, Seung Bum
Journal of the American Chemical Society, 2011 , vol. 133, # 17 p. 6642 - 6649
反应条件
1: diisobutyl aluminum hydride / tetrahydrofuran / -40 °C View Scheme
参考文献
West, Thomas H.; Daniels, David S. B.; Slawin, Alexandra M. Z.; Smith, Andrew D.
Journal of the American Chemical Society, 2014 , vol. 136, # 12 p. 4476 - 4479
反应条件
sodium tetrahydroborate; cerium(III) chloride
参考文献
Bondzic, Bojan P.; Eilbracht, Peter
Organic Letters, 2008 , vol. 10, # 16 p. 3433 - 3436
反应条件
C15H22Cl2N3O2PRu; glycerol; potassium hydroxide T=100°C; 6 h; Inert atmosphere;
参考文献
Diaz-Alvarez, Alba E.; Crochet, Pascale; Cadierno, Victorio
Catalysis Communications, 2011 , vol. 13, # 1 p. 91 - 96
反应条件
dichloro(.eta.3:.eta.2:.eta.3-dodeca-2,6,10-triene-1,12-diyl)ruthenium(IV); caesium carbonate; isopropyl alcohol T=82°C; 5 h; Inert atmosphere;
参考文献
Cadierno, Victorio; Crochet, Pascale; Francos, Javier; Garcia-Garrido, Sergio E.; Gimeno, Jose; Nebra, Noel
Green Chemistry, 2009 , vol. 11, # 12 p. 1992 - 2000
反应条件
1: MnO2 / acetone; CH2Cl2 2: H2 / Pd/C / methanol 3: Swern oxidating reagent View Scheme
参考文献
Kwon, Byoung-Mog; Lee, Seung-Ho; Cho, Young-Kwon; Bok, Song-Hae; So, Seung-Ho; Youn, Mi-Ran; Chang, Soo-Ik
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 19 p. 2473 - 2476
