1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride in tetrahydrofuran; mineral oil 0.5 h; Cooling with ice; 2: acetophenone in tetrahydrofuran; mineral oil T=20°C;
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1: With copper(l) iodide; trimethylsilyl trifluoromethanesulfonate; lithium chloride in tetrahydrofuran T=-78°C; 1 h; 2: With trifluoroacetic acid in tetrahydrofuran T=-78 - 20°C; Further stages.;
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