反应条件
1: LiAlH4, triethanol amine / diethyl ether; H2O / 2 h / Heating
2: 94 percent / NaH, MeOH / pentane; diethyl ether
3: 56 percent / xylene / 12 h / 140 °C
4: 43 percent / 6M NaOH / ethanol / 48 h
5: 97 percent / pyridine / diethyl ether / 48 h / Ambient temperature
6: 67 percent / diisopropylamine, phosphoryl chloride / CH2Cl2 / a) 1 h, 0 to 5 deg C, b) 1 h, r.t.
7: flash pyrolysis
View Scheme
参考文献
Wolber, Erwin K. A.; Schmittel, Michael; Ruechardt, Christoph
Chemische Berichte, 1992 , vol. 125, # 2 p. 525 - 532
